ガスクロマトグラフィーによる作物中の殺虫剤アセタミプリドおよび代謝物の総量分析法
-
- 時枝 正則
- Analysis of Chemicals & Pesticide Residue, Nisso Chemical Analysis Service Co., Ltd.
-
- 小澤 道弘
- Analysis of Chemicals & Pesticide Residue, Nisso Chemical Analysis Service Co., Ltd.
-
- 小林 茂
- Analysis of Chemicals & Pesticide Residue, Nisso Chemical Analysis Service Co., Ltd.
-
- 五明 健
- Analysis of Chemicals & Pesticide Residue, Nisso Chemical Analysis Service Co., Ltd.
書誌事項
- タイトル別名
-
- Method to Determination of Total Residues of the Insecticide Acetamiprid and Its Metabolites in Crops by Gas Chromatography
- Method to Determination of Total Residu
この論文をさがす
抄録
An analytical method has been developed for the determination of acetamiprid, (E)-N1-[(6-chloro-3-pyridyl)methyl]-N2-cyano-N1-methylacetamidine (ATP) and its metabolites, IM-2-1, IM-0, IC-0 and IM-0-Glucose in crops by gas chromatography (GC). ATP and its metabolites in crops were extracted with methanol and derivatized to methyl 6-chloronicotinate (IC-0-Me) through alkali hydrolysis, potassium permanganate oxidation and then esterification by diazomethane, followed by column chromatography clean-up and GC determination. The limit of detection was 0.01ppm and the recoveries of fortified samples ranged from 74 to 92%.
収録刊行物
-
- 日本農薬学会誌(Journal of Pesticide Science)
-
日本農薬学会誌(Journal of Pesticide Science) 22 (2), 77-83, 1997
日本農薬学会
- Tweet
詳細情報 詳細情報について
-
- CRID
- 1390001205209980672
-
- NII論文ID
- 110001712982
-
- NII書誌ID
- AN00196227
-
- ISSN
- 03851559
- 13490923
- 1348589X
-
- NDL書誌ID
- 4217962
-
- データソース種別
-
- JaLC
- IRDB
- NDL
- Crossref
- NDL-Digital
- CiNii Articles
-
- 抄録ライセンスフラグ
- 使用不可