Development of Mass Production of Ce0.9Gd0.1O1.95 Nanopowder with High-Sintering Characteristics

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  • 易焼結性Ｃｅ０．９Ｇｄ０．１Ｏ１．９５ナノ粒子の量産技術の開発
  • イショウケツセイ Ce0 9Gd0 1O1 95ナノ リュウシ ノ リョウサン ギジュツ ノ カイハツ

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Abstract

The mass production process of Ce0.9Gd0.1O1.95 (CGO) nanopowder with high-sintering characteristics has been studied. Although CGO powders were fabricated using a large scale coprecipitation bath with a capacity of 65 kg/batch, particle size distribution curve of this powder showed two peaks for the agglomeration and this powder showed lower sintering characteristics, compared to the CGO nanopowder by a small scale bath with a capacity of 0.1 kg/batch. It was found that when the impurity of NO3 - in the powder was removed by water using the rate of 50 L/kg, the formation of oval shape particles was observed and it is easy to crush the agglomerations in the powder by hammer-type mill. The sintering characteristics of this powder are almost same to those of the powder synthesized by the small scale bath.<br>

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