Synthesis and Crystal Structure of Bis{2-[(2-hydroxymethylphenyl)-iminomethyl]phenolato}chromium(III) nitrate monohydrate

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  • KOIKAWA Masayuki
    Department of Chemistry and Applied Chemistry, Faculty of Science and Engineering, Saga University
  • TOYOFUKU Takashi
    Department of Chemistry and Applied Chemistry, Faculty of Science and Engineering, Saga University
  • MUTO Masahiro
    Department of Chemistry and Applied Chemistry, Faculty of Science and Engineering, Saga University
  • YAMADA Yasunori
    Department of Chemistry and Applied Chemistry, Faculty of Science and Engineering, Saga University
  • TOKII Tadashi
    Department of Chemistry and Applied Chemistry, Faculty of Science and Engineering, Saga University

Description

The title compound, [CrIII(HL1-H)2]NO3·H2O, [H2L1-H = 2-[2-(hydroxymethylphenyl)iminomethyl)phenol], was synthesized and characterized by single-crystal X-ray analysis. The compound crystallizes in the triclinic system, space group P1 and Z = 2 with cell parameters a = 9.409(5)Å, b = 12.330(5)Å, c = 13.789(5)Å, α = 116.13(3)°, β = 96.99(4)°, γ = 104.81(4)°, V = 1337.1(11)Å3. The tridentate ligands bind to the chromium atom as monoanionic chelates.

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