In Situ Measurement of Composition in High-Temperature Solutions by X-Ray Fluorescence Spectrometry.

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  • Ujihara Toru
    Institute for Materials Research, Tohoku University, Aoba-ku, Sendai 980-8577, Japan
  • Sazaki Gen
    Institute for Materials Research, Tohoku University, Aoba-ku, Sendai 980-8577, Japan
  • Miyashita Satoru
    Institute for Materials Research, Tohoku University, Aoba-ku, Sendai 980-8577, Japan
  • Usami Noritaka
    Institute for Materials Research, Tohoku University, Aoba-ku, Sendai 980-8577, Japan
  • Nakajima Kazuo
    Institute for Materials Research, Tohoku University, Aoba-ku, Sendai 980-8577, Japan

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説明

We proposed an in situ technique based on X-ray fluorescence spectrometry to measure the composition of a high-temperature solution in a crucible. The sample holder for this technique was composed of carbon, which is transparent to X-rays. Using the present technique, equilibrium compositions of zinc in a gallium solution were measured. The results agreed well with the liquidus curve of the Ga–Zn phase diagram, and thus the validity of this technique was proved.

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