Preparation of Polyimides by Using Mixtures of Tetrahydrofuran and Methanol and Their Properties.

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説明

Reaction conditions of the preparation of solutions of polyamic acids in the tetrahydrofuran/methanol mixed solvent (THF/MeOH) were studied. The polyamic acids were based on pyromellitic dianhydride and 4,4’-oxydianiline. Transparent solutions were prepared at 5 wt% and lower concentrations of polyamic acid in the THF/MeOH mixture with component weight ratio ranging from 4:1 to 1:1. The properties of the final polyimide films were compared with those prepared by using N-methyl-2-pyrrolidone as the solvent.

収録刊行物

  • Polymer Journal

    Polymer Journal 34 (2), 54-56, 2002

    The Society of Polymer Science, Japan

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