Surface segregation of lead in high-purity aluminum.
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- TSUBAKINO Harushige
- Faculty of Engineering, Himeji Institute of Technology
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- TERASAWA Michitaka
- Faculty of Engineering, Himeji Institute of Technology
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- MITAMURA Tohru
- Faculty of Engineering, Himeji Institute of Technology
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- NOGAMI Atsushi
- Graduate School, Himeji Institute of Technology
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- SUGIMOTO Kiminori
- Showa Aluminium Co. LTD
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- KINOMURA Atsushi
- Osaka National Research Institute, AIST
Bibliographic Information
- Other Title
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- 高純度アルミニウム中の鉛の表面偏析
- コウジュンド アルミニウム チュウ ノ ナマリ ノ ヒョウメンヘンセキ
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Abstract
Surface segregation of Pb in the annealed Al-foils has been studied by Rutherford back scattering spectroscopy (RBS) and transmission electron microscopy (TEM). High-purity Al-foils containing 100 mass-ppm Pb were heat-treated for 1 h or 4 h at 540°C. Almost all of Pb segregate in a thin layer, 0.1 μm from the surface. Lead contents in the Pb-enriched surface layers were estimated to be 0.1∼0.14 at% Pb which were about 100–fold higher than the initial bulk concentration. TEM observations show that Pb-particles are formed at foil surfaces and their size increases from about 80 nm to 240 nm when final annealing time increases from 1 h to 4 h at 540°C. The Pb particles have a cube-cube orientation relationship with Al matrix and are bounded by {100} and {111} facets.
Journal
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- Journal of Japan Institute of Light Metals
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Journal of Japan Institute of Light Metals 51 (2), 98-102, 2001
The Japan Institute of Light Metals
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Details 詳細情報について
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- CRID
- 1390001206335158016
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- NII Article ID
- 10006253306
- 10007262806
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- NII Book ID
- AN00069773
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- COI
- 1:CAS:528:DC%2BD3MXhsl2qsb8%3D
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- ISSN
- 18808018
- 04515994
- http://id.crossref.org/issn/04515994
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- NDL BIB ID
- 5679952
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- Text Lang
- ja
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- Data Source
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- JaLC
- NDL
- Crossref
- CiNii Articles
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- Abstract License Flag
- Disallowed