Structural Clarification of Caulerpa Cell Wall .BETA.-1,3-Xylan by NMR Spectroscopy.

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  • Structural Clarification of Caulerpa Cell Wall β-1,3-Xylan by NMR Spectroscopy
  • Structural Clarification of Caulerpa Ce
  • Structural Clarification of<i>Caulerpa</i>Cell Wall/M,3-Xylan by NMR Spectroscopy

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^1H- and 13C-NMR spectroscopic analyses of cell wall microfibril β-1, 3-xylan from Caulerpa brachypus were performed in detail. The total assignment of all 1H- and 13C-NMR signals in the β-1, 3-xylan was achieved by evaluating the 2D C-H COSY, DQF-COSY, and NOESY spectra. The results, including information on through-space interaction between the xylopyranose residues, were confirmed. The determination of the glycosidic linkages by NMR spectroscopic analyses agrees well with the results from a chemical analysis.

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