Study on the Resolution of Latex-State NMR spectroscopy

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  • FUKUHARA Lina
    Department of Chemical Science and Engineering, Tokyo National College of Technology
  • MINOWA Jun
    Department of Materials Science and Technology, Nagaoka University of Technology
  • KOSUGI Kenichiro
    Department of Materials Science and Technology, Nagaoka University of Technology
  • YAMAMOTO Yoshimasa
    Department of Chemical Science and Engineering, Tokyo National College of Technology
  • ISHII Hiroyuki
    Department of Chemical Science and Engineering, Tokyo National College of Technology
  • KAWAHARA Seiichi
    Department of Materials Science and Technology, Nagaoka University of Technology

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Other Title
  • ラテックスNMRスペクトルの分解能に関する研究
  • ラテックス NMR スペクトル ノ ブンカイノウ ニ カンスル ケンキュウ

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Description

Resolution and relaxation time of latex-state nuclear magnetic resonance (NMR) spectroscopy were investigated with respect to not only the mobility of the polymer but also to the movement of the dispersoid in the latex. The latex was prepared by emulsion polymerization and soap-free polymerization of butyl acrylate with peroxodisulfate. The latex-state 13C NMR spectra were measured with various pulse sequences that were known to be useful for the solution state 13C NMR spectroscopy. The high resolution latex state NMR was achieved at a temperature of more than 78 K.

Journal

  • KOBUNSHI RONBUNSHU

    KOBUNSHI RONBUNSHU 72 (1), 22-30, 2015

    The Society of Polymer Science, Japan

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