Elution Behavior of Carbohydrates Using Core-Shell Ion-Exchange Resin St-70 with Different Degrees of Cross-Linking in the Porous Shell
-
- MITOMO Shun-ichi
- Institute of Nutrition Sciences, Kagawa Nutrition University
-
- INOUE Yutaka
- Faculty of Pharmacy and Pharmaceutical Sciences, Josai University
-
- TANIKAWA Takashi
- Faculty of Pharmacy and Pharmaceutical Sciences, Josai University
-
- NEGISHI Yukiko
- Institute of Nutrition Sciences, Kagawa Nutrition University
この論文をさがす
抄録
<p>A novel core-shell ion-exchange resin (St-70) having a core-shell monomer weight ratio of 30:70 was prepared for use in highperformance liquid chromatography (HPLC), and the effect of the degree of cross-linking (10–55%) of the porous shell on the separation of carbohydrates was examined. A mixture of inositol, glucose, fructose, and sucrose was separated under alkaline conditions (100 and 150 mmol/L NaOH) at flow rates of 0.3–0.7 mL/min using St-70, which exhibited a degree of cross-linking of 10, 40, and 55%. The retention time of carbohydrates decreased with increasing of the degree of cross-linking in the porous shell. The theoretical plate number (N) of glucose, fructose, and sucrose decreased with decreasing the degree of cross-linking when 100 mmol/L NaOH eluent was used at flow rates of 0.3 and 0.5 mL/min. </p>
収録刊行物
-
- CHROMATOGRAPHY
-
CHROMATOGRAPHY 44 (3), 151-155, 2023-10-20
クロマトグラフィー科学会
- Tweet
詳細情報 詳細情報について
-
- CRID
- 1390016572052392576
-
- NII書誌ID
- AA1137755X
-
- ISSN
- 13483315
- 13428284
-
- NDL書誌ID
- 033150652
-
- 本文言語コード
- en
-
- データソース種別
-
- JaLC
- NDL
- Crossref
-
- 抄録ライセンスフラグ
- 使用不可