Recent Advance in Structural Studies under Extreme Conditions. Single Crystal Structure Analysis under High Pressures Using Helium as a Pressure Transmitting Medium.

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  • MATSUSHITA Nobuyuki
    Department of Chemistry, Graduate School of Arts and Sciences, The University of Tokyo

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  • 特殊条件下の構造研究の新展開　　へリウムを圧力媒体とした高圧単結晶構造解析
  • ヘリウム オ アツリョク バイタイ ト シタ コウアツタンケッショウ コウゾウ カイセキ

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Abstract

In this paper, a technique of single-crystal X-ray diffraction measurements under high pressures, using a diamond anvil cell with helium gas as an inert and hydrostatic pressuretransmitting medium, is described. The technique has been applied to a three-dimensional halogen-bridged mixed-valence gold complex, CS2 [AuICl2] [AuIIICl4] to investigate the mixedvalence state and the crystal structure under high pressures up to 18 GPa.

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