ポーラログラフにる活字合金地金中の不純物の定量

高木 十郎, 角田 真好, 若林 和司

doi:10.11413/nig1958.6.69

書誌事項

タイトル別名

Polarographic Determination of the Impurities in Type Metal

説明

An experiment was made on D. C. polarographic determinstion of Fe, Zn etc., the most ifluential impurities upon type metal. The greater part of Pb can be removed as pbCl₂ by dissolving the sample in HCl-HNO₃ mixture. Then Cu, Fe, Zn were separated as sulphides by the action of K₂S from Sb, Sn in alkaline sample solution. The polarograms on 0--1.4V (vs, Hg pool) were ready to be taken.<br>The separation process took rather much time but polarograms obtained were good, and neither special reagent nor apparatus was needed. The mean error for each impurity was Cu-5%, Fe-4%, Zn-3%.

収録刊行物

日本印刷学会論文集

日本印刷学会論文集 6 (14), 69-72, 1963

社団法人日本印刷学会

詳細情報詳細情報について

CRID: 1390282679066227840

NII論文ID: 130004186456

DOI: 10.11413/nig1958.6.69

ISSN: 21851263; 00400874

データソース種別

JaLC
CiNii Articles

抄録ライセンスフラグ: 使用不可

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