Effect of polyether linkages on the carboxylation of sodium phenoxide.

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In the carboxylation of sodium phenoxide under mild conditions, the crown compound or polyethers with three to five ether linkages caused carboxylation to give o- and p-hydroxybenzoic acids, but not ethers with one or two linkages. The chelation of sodium phenoxide with polyethers changed the formation ratio of isomers.

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