Cyanamide derivatives. 106. The preparation of 15N-labeled cyanoguanidines.

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  • Omura Akira
    Department of Electronic Chemistry, The Graduate School, Tokyo Institute of Technology
  • Nonaka Tsutomu
    Department of Electronic Chemistry, The Graduate School, Tokyo Institute of Technology
  • Fuchigami Toshio
    Department of Electronic Chemistry, The Graduate School, Tokyo Institute of Technology
  • Ichikawa Eiichi
    Department of Electronic Chemistry, The Graduate School, Tokyo Institute of Technology
  • Odo Keijiro
    Department of Electronic Chemistry, The Graduate School, Tokyo Institute of Technology

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  • Cyanamide Derivatives. Part 106. The Preparation of 15N-Labeled Cyanoguanidines

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Methods for labeling the chemically non-equivalent nitrogen atoms of cyanoguanidine with 15N were established. 1-Cyanoguanidine-1-15N and 1-cyano-15N-guanidine were prepared, and their labeled positions were also confirmed by mass spectroscopic analysis. 15N FT-NMR spectra of cyanoguanidine enriched with 15N were measured.

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