The Methylenation of Several Allylbenzene-1,2-diol Derivatives in Aprotic Polar Solvents

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  • Fujita Harushige
    Department of Chemistry, Faculty of Science and Technology, Kinki University
  • Yamashita Masataro
    Department of Chemistry, Faculty of Science and Technology, Kinki University

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  • ChemInform Abstract: THE METHYLENATION OF SEVERAL ALLYLBENZENE‐1,2‐DIOL DERIVATIVES IN APROTIC POLAR SOLVENTS

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The aprotic polar solvents, such as DMF (N,N-dimethylformamide) and DMSO (dimethyl sulfoxide), accelerated very effectively the methylenation of 1,2-dihydroxy-4- (I), 1,2-dihydroxy-3,4-dimethoxy-5- (II), and 1,2-dihydroxy-3-methoxy-5-allylbenzene (III) in the presence of bronze and cupric oxide as catalysts.

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