New Entry of Coupling Reaction of Phenacylamine Derivatives with Silylstannane.
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- Iwai Yasumasa
- Graduate School of Pharmaceutical Sciences, The University of Tokushima
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- Kita Kumiko
- Graduate School of Pharmaceutical Sciences, The University of Tokushima
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- Matsushita Yoko
- Graduate School of Pharmaceutical Sciences, The University of Tokushima
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- Yamauchi Aiko
- Graduate School of Pharmaceutical Sciences, The University of Tokushima
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- Kihara Masaru
- Graduate School of Pharmaceutical Sciences, The University of Tokushima
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説明
The new coupling reaction of phenacylamines with silylstannane and lithium diisopropylamide (LDA) is reported. The treatment of a phenacylamine iodide 1 with (trimethylsilyl)tributylstannane (Me3SiSnBu3) and cesium fluoride (CsF) gave a dimerization product 2 having no iodine atom. Reaction of 1 with LDA afforded a dimerization product 3 with an iodine atom. The products 2 and 3 were separated to the meso and racemic isomers, respectively.
収録刊行物
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- CHEMICAL & PHARMACEUTICAL BULLETIN
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CHEMICAL & PHARMACEUTICAL BULLETIN 50 (3), 441-443, 2002
公益社団法人 日本薬学会
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詳細情報 詳細情報について
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- CRID
- 1390282679138855808
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- NII論文ID
- 110003616175
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- NII書誌ID
- AA00602100
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- COI
- 1:CAS:528:DC%2BD38Xks12ktLk%3D
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- ISSN
- 13475223
- 00092363
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- NDL書誌ID
- 6263565
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- PubMed
- 11911219
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
- Crossref
- PubMed
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可