Preparation of 2,2-difluoro- and 2,2,4.ALPHA.-trifluoro-steroids by the reaction of enamines with perchloryl fluoride.

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The reaction of fluorinated steroidal enamines with perchloryl fluoride furnished 2, 2-difluoro-and 2, 2, 4α-trifluorinated steroids. Changes in infrared absorption frequency due to the introduction of fluorine are discussed.

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