高速液体クロマトグラフィーによるごま油中のセサモリン, セサミンの定量及びセサモールの確認

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書誌事項

タイトル別名
  • Determination of Sesamolin, Sesamin and Sesamol in Sesame Oil by High Performance Liquid Chromatography
  • コウソク エキタイ クロマトグラフィー ニヨル ゴマユチュウ ノ セサモリン
公開日
1982
DOI
  • 10.3358/shokueishi.23.142
公開者
公益社団法人 日本食品衛生学会

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説明

A high performance liquid chromatographic (HPLC) method was established for the quantitative determination of sesamolin, sesamin and sesamol in sesame oil.<br>Sesamolin, sesamin and sesamol were eluted at approximately 8min, 13min and 35min by using a 4.6mm∅×250mm Lichrosorb-Si 60 column with n-hexane·chloroform (80:20). The ultraviolet absorption detector was set at 280nm. Sesame oil was diluted with the eluting solvent and a sample was directly injected into the HPLC machine.<br>The results were as follows:<br>1. The extracted sesame oil were found to contain 0.42% sesamolin and 0.54% sesamin.<br>2. No sesamol was detected in a survey of sesame oil by this procedure (detection limit 0.0005%).<br>3. The average recoveries of sesamolin, sesamin and sesamol from sesame oil were 99.3%, 97.3%, 99.0%, respectively.

収録刊行物

  • 食品衛生学雑誌

    食品衛生学雑誌 23 (2), 142-148_1, 1982

    公益社団法人 日本食品衛生学会

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