A Sensitive Analytical Method for Six Aflatoxins in Rainbow Trout Muscle and Liver
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- OGISO Motoki
- Japan Food Research Laboratories, Tama Laboratory
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- KIMURA Ayako
- Japan Food Research Laboratories, Tama Laboratory
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- CHIKASOU Masato
- Japan Food Research Laboratories, Tama Laboratory
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- SAITO Maki
- Japan Food Research Laboratories, Tama Laboratory
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- TAKEMOTO Masami
- Japan Food Research Laboratories, Tama Laboratory
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- WATAI Masatoshi
- Japan Food Research Laboratories, Tama Laboratory
Bibliographic Information
- Other Title
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- ニジマスの筋肉および肝臓中の６種のアフラトキシン類の高感度分析
- ニジマス ノ キンニク オヨビ カンゾウ チュウ ノ 6シュ ノ アフラトキシンルイ ノ コウカンド ブンセキ
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Abstract
A highly sensitive analysis method for six aflatoxins (aflatoxin B1, B2, G1, G2, M1 and aflatoxicol) in rainbow trout muscle and liver was developed. Aflatoxins (AFs) were extracted with acetonitrile-water (9 : 1), purified on an immunoaffinity column, and subjected to HPLC with fluorescence detection after post-column photochemical derivatization. The recoveries of AFs at 0.05 μg/kg spiking levels were 71.4-82.4% in muscle and 80.1-93.0% in liver, and the repeatability relative standard deviations (RSDr) were 0.87-4.6% in muscle and 2.0-6.2% in liver. Limits of quantitation (LOQs) and limits of detection(LODs)of AFs were estimated to be 0.004-0.029 μg/kg, and 0.002-0.012 μg/kg, respectively.
Journal
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- Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)
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Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 52 (3), 161-166, 2011
Japanese Society for Food Hygiene and Safety
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Details 詳細情報について
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- CRID
- 1390282679202736896
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- NII Article ID
- 130000909922
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- NII Book ID
- AN00117741
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- COI
- 1:CAS:528:DC%2BC3MXpsVyms7Y%3D
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- ISSN
- 18821006
- 00156426
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- NDL BIB ID
- 11166910
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- PubMed
- 21720121
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- Text Lang
- ja
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- Data Source
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- JaLC
- IRDB
- NDL
- Crossref
- PubMed
- CiNii Articles
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- Abstract License Flag
- Disallowed
