Trace Analysis of Lead in Copper Gluconate by Atomic Absorption Spectrometry after Separation by Co-Precipitation with Bismuth
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- ITO Michio
- Japan Food Research Laboratories
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- ISHIGURO Satoshi
- Japan Food Research Laboratories
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- TAKAHASHI Fumihito
- Japan Food Research Laboratories
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- NOMURA Takakazu
- Japan Food Research Laboratories
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- SUGIMOTO Toshiaki
- Japan Food Research Laboratories
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- NISHIMURA Tsutomu
- Japan Food Research Laboratories
Bibliographic Information
- Other Title
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- ビスマス共沈分離–原子吸光光度法によるグルコン酸銅中の鉛の微量分析
- ビスマス キョウチン ブンリ-ゲンシ キュウコウ コウドホウ ニ ヨル グルコンサン ドウ チュウ ノ ナマリ ノ ビリョウ ブンセキ
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Abstract
In order to determine trace amounts of lead in copper gluconate by atomic absorption spectrometry (AAS), the authors investigated a separation and pre-concentration procedure using a co-precipitation technique with bismuth. After ashing 2.0 g of the sample by means of a dry process, the ash was dissolved in (1→100) nitric acid and 75 μg of bismuth was added. Lead was co-precipitated by using an ammonium solution controlled to pH 9.5–10.5. The precipitate was left at room temperature for over 15 minutes to age, and then washed with a (3→100) ammonium solution three times. The precipitate was dissolved in (1→100) nitric acid and then analyzed by AAS. The quantification limit of this method was 0.5 mg/kg, and the trueness, repeatability and intermediate precision were 99.6%, 4.2% and 4.2% at the spiked concentration of 0.5 mg/kg, and 94.4%, 2.8% and 4.0% at the spiked concentration of 5.0 mg/kg, respectively. Thus, the present method for trace analysis of lead in copper gluconate was validated.
Journal
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- Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)
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Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 56 (3), 114-117, 2015
Japanese Society for Food Hygiene and Safety
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Details 詳細情報について
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- CRID
- 1390282679204590848
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- NII Article ID
- 130005087128
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- NII Book ID
- AN00117741
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- ISSN
- 18821006
- 00156426
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- NDL BIB ID
- 026594889
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- PubMed
- 26156167
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- Text Lang
- ja
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- Data Source
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- JaLC
- IRDB
- NDL
- Crossref
- PubMed
- CiNii Articles
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- Abstract License Flag
- Disallowed