Direct Hydrothermal Synthesis of Size-Controlled Co₃O₄ Nanocubes under Highly Condensed Conditions
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- Kanie Kiyoshi
- Institute of Multidisciplinary Research for Advanced Materials, Tohoku University
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- Tsujikawa Yusuke
- Institute of Multidisciplinary Research for Advanced Materials, Tohoku University
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- Muramatsu Atsushi
- Institute of Multidisciplinary Research for Advanced Materials, Tohoku University
書誌事項
- タイトル別名
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- Direct Hydrothermal Synthesis of Size-Controlled Co<sub>3</sub>O<sub>4</sub> Nanocubes under Highly Condensed Conditions
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<p>Cobalt oxide (Co3O4) nanocubes with high crystallinity and a narrow size distribution have been synthesized in one pot process under highly condensed hydrothermal reactions using cobalt(II) nitrate (Co(NO3)2) and sodium hydroxide or tetramethylammonium hydroxide. The particle morphology was controlled to a cubic shape by change in the initial pH. The particle mean diameter was also gradually controlled by the change in the initial pH in the range from 18 nm to 66 nm. Co(OH)2 hexagonal thin platelet particles were obtained as the predominant product when CoSO4, CoCl2, and Co(CH3COO)2 were used as the Co-source. The result indicated that oxidation ability of nitrate anions played an important role to obtain the Co3O4 nanocubes in the one pot process.</p>
収録刊行物
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- MATERIALS TRANSACTIONS
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MATERIALS TRANSACTIONS 58 (7), 1014-1019, 2017
公益社団法人 日本金属学会
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詳細情報 詳細情報について
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- CRID
- 1390282679229863808
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- NII論文ID
- 130006777003
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- NII書誌ID
- AA1151294X
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- ISSN
- 13475320
- 13459678
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- NDL書誌ID
- 028315354
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
- Crossref
- CiNii Articles
- KAKEN
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- 抄録ライセンスフラグ
- 使用不可