Preparation of Ni-Aluminide Surface Layer Containing Hafnium by Molten-Salt Electrodeposition and Cyclic-Oxidation Resistance
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- Tabata Kazuki
- Department of Materials Science and Engineering, Graduate School of Engineering and Resource Science, Akita University
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- Fujii Hisato
- Department of Materials Science and Engineering, Graduate School of Engineering and Resource Science, Akita University
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- Sato Naka
- Department of Materials Science and Engineering, Graduate School of Engineering and Resource Science, Akita University
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- Hara Motoi
- Department of Materials Science and Engineering, Graduate School of Engineering and Resource Science, Akita University
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Abstract
The preparation of a coating consisting of Ni aluminide containing a small amount of Hf was carried out by the electrodeposition of Ni using an aqueous solution and the electrodeposition of Hf and Al using a molten salt. Furthermore, in order to change the depth of the layer containing Hf in the coating, a four-step electrodeposition of Ni, Hf, Ni and Al was carried out, and the times of the first and third Ni electrodepositions were changed. As a result, coatings consisting of Ni aluminide, which contained different depths of the Hf-containig layer, were formed. The cyclic-oxidation resistance of these specimens was evaluated in air at 1423 K. For the specimen with a shallow Hf-containing layer in the coating, the specimen mass reduction due to spallation of the scale was observed, whereas for the specimen with a deep Hf-containing layer, the specimen mass reduction was only slightly observed and a high-cyclic oxidation resistance was obtained. Among the specimens with a deep Hf-containing layer, the specimen prepared by Hf deposition for 0.6 ks showed the highest cyclic-oxidation resistance. For this specimen, the scale formed on the coating after the oxidation test consisted of Al2O3. This scale was adhesive, and locally entered the metal substrate.
Journal
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- MATERIALS TRANSACTIONS
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MATERIALS TRANSACTIONS 55 (8), 1311-1318, 2014
The Japan Institute of Metals and Materials
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Details 詳細情報について
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- CRID
- 1390282679229868160
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- NII Article ID
- 130004825191
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- NII Book ID
- AA1151294X
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- ISSN
- 13475320
- 13459678
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- NDL BIB ID
- 025617376
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- Text Lang
- en
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- Data Source
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- JaLC
- NDL
- Crossref
- CiNii Articles
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- Abstract License Flag
- Disallowed