Local Structural Analysis on Decomposition Process of LiAl(ND₂)₄

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  • Ikeda Kazutaka
    Institute of Materials Structure Science, KEK
  • Otomo Toshiya
    Institute of Materials Structure Science, KEK Department Materials Structure Science, The Graduate University for Advanced Studies
  • Ohshita Hidetoshi
    Institute of Materials Structure Science, KEK
  • Kaneko Naokatsu
    Institute of Materials Structure Science, KEK
  • Tsubota Masami
    Institute of Materials Structure Science, KEK
  • Suzuya Kentaro
    J-PARC Center, Japan Atomic Energy Agency
  • Fujisaki Fumika
    Department Materials Structure Science, The Graduate University for Advanced Studies
  • Ono Taisuke
    Graduate School of Advanced Sciences of Matter, Hiroshima University
  • Yamanaka Toshiyuki
    Graduate School of Advanced Sciences of Matter, Hiroshima University
  • Shimoda Keiji
    Institute for Advanced Materials Research, Hiroshima University
  • Ichikawa Takayuki
    Graduate School of Advanced Sciences of Matter, Hiroshima University Institute for Advanced Materials Research, Hiroshima University
  • Kojima Yoshitsugu
    Graduate School of Advanced Sciences of Matter, Hiroshima University Institute for Advanced Materials Research, Hiroshima University

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タイトル別名
  • Local Structural Analysis on Decomposition Process of LiAl(ND<sub>2</sub>)<sub>4</sub>

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Local structural changes that accompany amorphization during the decomposition of LiAl(ND2)4 were investigated by neutron total scattering measurements. Structure factors before the decomposition were attributed to single-phase LiAl(ND2)4 characterized by isolated [ND2] units. Atomic pair distribution functions after heat treatments at 433 and 673 K showed that LiAl(ND2)4 decomposed to amorphous mixed phases that contain Li3AlN2 and AlN.

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