Ag Nanoparticles-enhanced Fluorescence of Terbium-Deferasirox Complexes for the Highly Sensitive Determination of Deferasirox
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- ABOLHASANI Jafar
- Department of Chemistry, Tabriz Branch, Islamic Azad University
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- NADERALI Roza
- Department of Chemistry, Tabriz Branch, Islamic Azad University
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- HASSANZADEH Javad
- Department of Chemistry, Tabriz Branch, Islamic Azad University
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We describe the effect of different sized gold and silver nanoparticles on the terbium sensitized fluorescence of deferasirox. It is indicated that silver nanostructures, especially 18 nm Ag nanoparticles (AgNPs), have a remarkable amplifying effect compared to Au nanoparticles. Based on this observation, a highly sensitive and selective method was developed for the determination of deferasirox. Effects of various parameters like AgNPs and Tb3+ concentration and pH of media were investigated. Under the optimal conditions, a calibration curve was plotted as the fluorescence intensities versus the concentration of deferasirox in the range of 0.1 to 200 nmol L−1, and detection limit of 0.03 nmol L−1 was obtained. The method has good linearity, recovery, reproducibility and sensitivity, and was satisfactorily applied for the determination of deferasirox in urine and pharmaceutical samples.
収録刊行物
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- Analytical Sciences
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Analytical Sciences 32 (4), 381-386, 2016
社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390282679235585536
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- NII論文ID
- 130005143827
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- NII書誌ID
- AA10500785
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- ISSN
- 13482246
- 09106340
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- NDL書誌ID
- 027244965
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- PubMed
- 27063708
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
- Crossref
- PubMed
- CiNii Articles
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- 使用不可