Determination of Salicylic Acid in Human Serum and Urine Samples by High-Performance Liquid Chromatography with Post-column Ru(bipy)₃²⁺-Ce(SO₄)₂ Chemiluminescence Detection
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- LONG Xingyu
- School of Chemistry and Chemical Engineering of Southwest University Editorial Department of Journal of Guizhou Normal University
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- CHEN Funan
- School of Chemistry and Chemical Engineering of Southwest University
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- DENG Mao
- School of Chemistry and Chemical Engineering of Southwest University
書誌事項
- タイトル別名
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- Determination of Salicylic Acid in Human Serum and Urine Samples by High-Performance Liquid Chromatography with Post-column Ru(bipy)<sub>3</sub><sup>2+</sup>–Ce(SO<sub>4</sub>)<sub>2</sub> Chemiluminescence Detection
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A sensitive, novel and rapid chemiluminescence (CL) method combined with high-performance liquid chromatography (HPLC) separation for the determination of salicylic acid (SA) is described in this work. The method was based on the fact that SA could significantly enhance the CL of the reaction of cerium sulfate and the tris(2,2-bipyridyl) ruthenium(II) CL system in the presence of acid. Under the optimal conditions, the CL intensity was linear over concentrations of SA in the range of 0.02 – 10 × 10−6 g/mL, with a detection limit of 8 × 10−9 g/mL (S/N = 3). Also, the relative standard detection was 2.2% for 1.0 × 10−7 g/mL (n = 11). The proposed method has been successfully applied to the analysis of SA in human serum samples and urine samples with satisfactory results.
収録刊行物
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- Analytical Sciences
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Analytical Sciences 29 (2), 227-231, 2013
社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390282679237435904
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- NII論文ID
- 10031156860
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- NII書誌ID
- AA10500785
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- COI
- 1:STN:280:DC%2BC3sznsVehtA%3D%3D
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- ISSN
- 13482246
- 09106340
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- NDL書誌ID
- 024257974
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- PubMed
- 23400289
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- Web Site
- https://ndlsearch.ndl.go.jp/books/R000000004-I024257974
- https://link.springer.com/content/pdf/10.2116/analsci.29.227.pdf
- https://link.springer.com/article/10.2116/analsci.29.227/fulltext.html
- https://www.jstage.jst.go.jp/article/analsci/29/2/29_227/_pdf
- https://search.jamas.or.jp/link/ui/2013249111
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
- Crossref
- PubMed
- CiNii Articles
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