フタル酸エステル類の電子捕獲型検出器への応答
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- 柏平 伸幸
- 環境庁公害研修所
書誌事項
- タイトル別名
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- Response of phthalic acid esters to electron capture detector.
- フタルサン エステルルイ ノ デンシ ホカクガタ ケンシュツキ ヘ ノ オウト
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抄録
In order to obtain the optimal conditions for analysis of phthalic acid esters(PAEs) by GC-ECD, a response of di-2-ethylhexyl phthalate(DEHP) to ECD, on behalf of PAEs, was investigated with respect to column temperature and carrier gas flow rate. GC analysis was performed with Shimadzu GC-6A and ECD detection was conducted at 250 °C in the constant voltage mode. Among parameters in GC analysis, a carrier gas flow rate gave anomalous behaviors in ECD response. For example one noted response was an exponential decrease with an increase of flow rate. Furthermore a negative peak was observed at flow rates greater than 60 ml/min. The possible GC conditions for PAEs' analysis are recommended.
収録刊行物
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- 分析化学
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分析化学 36 (10), T103-T107, 1987
公益社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390282679330681088
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- NII論文ID
- 110002909487
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- NII書誌ID
- AN00222633
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- NDL書誌ID
- 3156623
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- ISSN
- 05251931
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- 本文言語コード
- ja
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- データソース種別
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- JaLC
- NDL
- Crossref
- NDL-Digital
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可