Determination of Melamine using LC-MS and Applications to Samples Related to Waste

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  • ＬＣ‐ＭＳを用いたメラミン定量法と廃棄物関連試料への適用
  • LC MS オ モチイタ メラミン テイリョウホウ ト ハイキブツ カンレン シリョウ エ ノ テキヨウ

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Abstract

Melamine (2, 4, 6-triamino-1, 3, 5-triazine), a raw material of Melamine resin is considered to be an organic pollution source in environment. We developed a determination method for Melamine by LC-MS, and applied the method to liquid samples such as leachate. Target compounds were extracted with a solid phase cartridge. Method Detection Limit was calculated from the standard deviation of the result of seven replicates. The Calculated MDL, average recovery ratio and RSD was 0.018μg/l 93.4% and 2.5%, respectively. On a quantity analysis of waste related samples, the melamine was detected from all the samples tested.

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