Occupational Exposure to Aromatic Hydrocarbons at a Coke Plant: Part 1. Identification of Hydrocarbons in Air and their Metabolites in Urine by a Gas Chromatography-Mass Spectrometry Method
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- Bieniek Grazyna
- Department of Molecular Biology, Biochemistry and Biopharmacy, Faculty of Pharmacy, Medical University of Silesia
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- Kurkiewicz Slawomir
- Department of Molecular Biology, Biochemistry and Biopharmacy, Faculty of Pharmacy, Medical University of Silesia
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- Wilczok Tadeusz
- Department of Molecular Biology, Biochemistry and Biopharmacy, Faculty of Pharmacy, Medical University of Silesia
書誌事項
- タイトル別名
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- Occupational Exposure to Aromatic Hydrocarbons at a Coke Plant: Part I. Identification of Hydrocarbons in Air and their Metabolites in Urine by a Gas Chromatography-Mass Spectrometry Method
- Occupational Exposure to Aromatic Hydrocarbons at a Coke Plant: Part I. Identification of Hydrocarbons in Air and their Metabolites in Urine by a Gas Chromatography‐Mass Spectrometry Method
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A method for the qualitative analysis of aromatic hydrocarbons in air and their various urinary metabolites is presented. The air was sampled in charcoal tubes and extracted with carbon disulfide. The hydrocarbons were identified as being aliphatic hydrocarbons (C9-C19), aromatic hydrocarbons and heterocyclic compounds. The urinary metabolites after enzymatic hydrolysis were analyzed by solid-phase extraction with a styrene-divinylbenzene resin, silylation with N,O-bis(trimethylsilyl)acetamide and GC/MS for separation and detection. Satisfactory separation of all compounds investigated was achieved without interference due to matrix peaks. The following compounds were identified in the urine of workers: dimethylphenol isomers, 4-ethyl-1,3-benzenediol, 2-ethoxybenzoic acid and methoxyphenols. Trimethylsilyl derivatives of aromatic hydroxyacids and hydroxymethoxyacids were found in the urine of occupationally exposed workers by means of a silylation procedure.<br>
収録刊行物
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- journal of Occupational Health
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journal of Occupational Health 46 (3), 175-180, 2004
公益社団法人 日本産業衛生学会
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詳細情報 詳細情報について
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- CRID
- 1390282679433540224
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- NII論文ID
- 130004447198
- 110003722939
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- NII書誌ID
- AA11090645
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- COI
- 1:CAS:528:DC%2BD2cXlsFynsLk%3D
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- ISSN
- 13489585
- 13419145
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- NDL書誌ID
- 6961658
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- PubMed
- 15215657
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
- Crossref
- PubMed
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可