スパーク放電発光分析における介在物選択放電過程の高速度カメラによるその場観察

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書誌事項

タイトル別名
  • In-situ Observation on the Explosion Process of Inclusions in Spark OES Analysis Using High Speed Camera
  • スパーク ホウデン ハッコウ ブンセキ ニ オケル カイザイブツ センタク ホウデン カテイ ノ コウソクド カメラ ニ ヨル ソノバ カンサツ

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説明

The Spark electric discharge optical emission spectrometry has been widely applied to a rapid composition analysis of molten elements in the field of steel making processes. The advantage of this method is that the simultaneously composition analysis from light elements to heavy ones is possible and that the acid soluble elements and insoluble inclusions can be analyzed separately. In this study, spark phenomena in discharge and sample surface morphology were investigated using high-speed camera, SEM-EDS, and spark-OES methods. On the basis of detailed analyses of spark images between electrode and sample surfaces, it was found that the explosion process of inclusion consists of the following three stages. At first, a breakdown between sample surface and electrode occurs, and then inclusions are transformed to cathode points. Finally, vapor jet spouts out to electrode and collides with electrons, Ar+, and Ar* leading to strong plasma light. In this process plural inclusions are initially destroyed and dispersed finely into the matrix. These findings led us a new model for the selective discharge of inclusions in spark discharge.

収録刊行物

  • 鉄と鋼

    鉄と鋼 94 (11), 532-538, 2008

    一般社団法人 日本鉄鋼協会

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