A New Method for Preparing Monolithic Gels as Precursor for M<sub><i>x</i></sub>O<sub><i>y</i></sub> and SiO<sub>2</sub>-M<sub><i>x</i></sub>O<sub><i>y</i></sub> Glasses (M=Al, Ti, Zr) of an Arbitrary

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  • ABE Yoshimoto
    Department of Industrial Chemistry, Faculty of Science and Technology, Science University of Tokyo
  • SUGIMOTO Noriyasu
    Department of Industrial Chemistry, Faculty of Science and Technology, Science University of Tokyo
  • NAGAO Yukinori
    Department of Industrial Chemistry, Faculty of Science and Technology, Science University of Tokyo
  • MISONO Takahisa
    Department of Industrial Chemistry, Faculty of Science and Technology, Science University of Tokyo

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  • M<sub><i>x</i></sub>O<sub><i>y</i></sub>及び任意の組成を有するSiO<sub>2</sub>-M<sub><i>x</i></sub>O<sub><i>y</i></sub>ガラス前駆体としての均一ゲルの新規合成法
  • MxOy オヨビ ニンイ ノ ソセイ オ ユウスル SiO2 MxOy ガラス

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Abstract

A new method for preparing gels as a precursor for SiO2-MxOy (M=Al, Ti, Zr) glasses of an arbitrary composition was investigated. The gels were formed via polymetalloxanes from hydrolytic condensation of metal chelates of ethyl acetoacetate or condensation polymerization of the chelate with silicic acid. The method permitted to prepare transparent gel plates of MxOy and binary SiO2-MxOy component systems.

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