ジャスモン酸メチルの工業化技術の開発

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  • Development of methyl(.+-.)-jasmonate production process on an industrial scale.
  • ジャスモンサン メチル ノ コウギョウカ ギジュツ ノ カイハツ

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An economical synthetic process of methyl jasmonate has been established.<BR>Total yield of this process is higher than 60 % for all five steps from cheaply available adipic acid. 2-Pentyny1-2-cyclopentenone, the key intermediate in this route, is synthesized by applying the improved palladiumcatalyzed enone formation from allyl β-keto carboxylate as a key reaction. The pentynyl moiety is introduced by the use of pentynyl chloride which is prepared in two steps from 2-butyne, our original source, cheaply.

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