書誌事項
- タイトル別名
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- Studies on Sulphur in Acetylene Gas Generated by Dry Type Generators and Method of Gas Purification
- カンシキ アセチレンガス チュウ ノ イオウ ト ガス セイジョウホウ
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Removal of sulfur components by washing with a dilute sodium hypochlorite solution from acetylene generated in a dry type generator has been studied.<BR>Calcium carbide containing more than 1 wt% calcium sulfide gave crude acetylene which contained sulfur components at a level of 1 × 10-1-1 × 10-2 vol% calculated as hydrogen sulfide. The white crystal extracted from the precipitates in the mist separator after purification was found to be α, β, α', β'-tetrachlorodiethyl sulfoxide. Optimum pH of the purification solution was 7.3-6.5, and the effect of the chlorine content was also clarified. Pre-washing of crude acetylene with 10% aqueous sodium hydroxide before the treatment with the sodium hypochlorite proved very effectivefor the removal of hydrogen sulfide.
収録刊行物
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- 有機合成化学協会誌
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有機合成化学協会誌 27 (4), 345-351, 1969
公益社団法人 有機合成化学協会
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詳細情報 詳細情報について
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- CRID
- 1390282680289538944
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- NII論文ID
- 130000930621
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- NII書誌ID
- AN0024521X
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- ISSN
- 18836526
- 00379980
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- NDL書誌ID
- 8466704
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- データソース種別
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- JaLC
- NDL
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