書誌事項
- タイトル別名
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- Syntheses of Amphiphiles Containing Two Azobenzene Units in a Molecule
- 1 ブンシナイ ニ アゾベンゼン タンイ オ 2コ ユウスル リョウシンバイセ
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説明
Five new amphiphiles each containing two azobenzene units in a molecule were synthesized through four reaction steps. The first step was azo-coupling reactions with aniline derivatives and phenol. The second step was Williamson etherification reaction between sodium salts of phenols containing an azobenzene unit with ω-halogenated alcohols, such as 2-bromoethanol or 3-chloro-l-propanol. The third step was diesterification reactions between alcohols having an azobenzene unit and maleic anhydride, the diester of maleic acid containing two azobenzene units in a molecule was obtained. The fourth step was addition reaction of sodium hydrogensulfite with diesters. The products were characterized by 1H-NMR, IR, and Mass spectra.
収録刊行物
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- 油化学
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油化学 44 (12), 1075-1085, 1995
公益社団法人 日本油化学会
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詳細情報 詳細情報について
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- CRID
- 1390282680312075776
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- NII論文ID
- 10001754977
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- NII書誌ID
- AN00245435
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- ISSN
- 0513398X
- 18842003
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- NDL書誌ID
- 3640616
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- データソース種別
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- JaLC
- NDL
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- 抄録ライセンスフラグ
- 使用不可