Synthesis and Properties of Novel Fluorinated Polymethacrylates

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  • HAYAKAWA Yoshio
    National Industrial Research Institute of Nagoya, Chemistry Department, Fluorine Chemistry Laboratory
  • TERASAWA Naohiro
    National Industrial Research Institute of Nagoya, Chemistry Department, Fluorine Chemistry Laboratory
  • HAYASHI Eiji
    National Industrial Research Institute of Nagoya, Chemistry Department, Fluorine Chemistry Laboratory
  • ABE Takashi
    National Industrial Research Institute of Nagoya, Chemistry Department, Fluorine Chemistry Laboratory

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  • 新規な含フッ素ポリメタクリル酸エステルの合成と性質
  • シンキ ナ ガン フッソ ポリメタクリルサン エステル ノ ゴウセイ ト セイ

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Abstract

Novel fluorinated methacrylic polymers and copolymers were prepared. Perfluoroacid fluorides containing a dialkylamino group such as pyrrolidino and dipropylamino groups were reduced to the corresponding 1, 1-dihydroperfluoroalcohols, which were then reacted with methacryloyl chloride to give the methacrylates. The homopolymers and the copolymers with methyl methacrylate were obtained by a radical polymerization. The tough polymer films prepared by solution casting showed excellent water repellency with marked contact angle.

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