Preparation and Analysis of Alkyldibenzothiophenes.

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  • MIKI Yasuo
    National Institute of Advanced Industrial Science and Technology
  • SUGIMOTO Yoshikazu
    National Institute of Advanced Industrial Science and Technology
  • TANAKA Motoo
    Advanced Technology & Research Inst., Petroleum Energy Center, c/o National Inst. of Advanced Ind. Science & Technology
  • WU Zhiheng
    National Institute of Advanced Industrial Science and Technology

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  • アルキルジベンゾチオフェン類の調製および分析
  • アルキルジベンゾチオフェンルイ ノ チョウセイ オヨビ ブンセキ

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Abstract

By preparing and introducing dibenzothiophene (DBT), 4-methyl-DBT, 4, 6-dimethyl-DBT, and 2, 8-dimethyl-DBT, methyl-group, ethyl-group, propyl-group, isopropyl-group, and 110 of substituted DBT were obtained. The major compounds prepared were methyl-, dimethyl-, trimethyl-, tetramethyl-, pentamethyl-, hexamethyl, ethyl-, diethyl-, triethyl-, ethyl-methyl-, diethyl-methyl-, and ethyl-dimethyl-DBTs. Retention indices and characteristics in the mass spectra (ratio of the largest fragment ion to the parent ion) were measured for each compound.

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