Vitamin A Determination in Milk Samples Based on the Luminol-Periodate Chemiluminescence System
-
- RISHI Lubna
- Department of Chemistry, University of Balochistan
-
- YAQOOB Mohammad
- Department of Chemistry, University of Balochistan
-
- WASEEM Amir
- Department of Chemistry, Quaid-i-Azam University
-
- NABI Abdul
- Department of Chemistry, University of Balochistan
この論文をさがす
説明
A simple and rapid flow injection (FI) method for the determination of retinyl acetate is reported based on its enhancing effect on the luminol-periodate chemiluminescence (CL) system in an alkaline medium. The detection limit (3s×blank) was 8.0×10−8 mol L−1, with an injection throughput of 90 h−1. The method allows linear increase of CL intensity over the retinyl acetate concentration range of 1.0-100×10−7 mol L−1 (R2=0.9996) with relative standard deviations of 2.4% (n=10) for 5.0×10−7 mol L−1. The key chemical and physical variables (reagent concentrations, flow rates, sample volume, and photomultiplier tube (PMT) voltage) were optimized and potential interferences were investigated. The method was successfully applied to human milk, fresh cow's milk and infant milk-based formulas and the results were in good agreement with the previously reported HPLC method. A brief discussion on the possible CL reaction mechanism is also presented.
収録刊行物
-
- Ｊｏｕｒｎａｌ ｏｆ Ｎｕｔｒｉｔｉｏｎａｌ Ｓｃｉｅｎｃｅ ａｎｄ Ｖｉｔａｍｉｎｏｌｏｇｙ
-
Ｊｏｕｒｎａｌ ｏｆ Ｎｕｔｒｉｔｉｏｎａｌ Ｓｃｉｅｎｃｅ ａｎｄ Ｖｉｔａｍｉｎｏｌｏｇｙ 60 (1), 9-16, 2014
一般財団法人 学会誌刊行センター
- Tweet
詳細情報 詳細情報について
-
- CRID
- 1390282681301897600
-
- NII論文ID
- 130003393768
-
- NII書誌ID
- AA00703822
-
- COI
- 1:CAS:528:DC%2BC2cXkvV2nu7g%3D
-
- ISSN
- 18817742
- 03014800
-
- NDL書誌ID
- 025307449
-
- PubMed
- 24759254
-
- 本文言語コード
- en
-
- データソース種別
-
- JaLC
- NDL
- Crossref
- PubMed
- CiNii Articles
-
- 抄録ライセンスフラグ
- 使用不可
