Crystal Structure of <i>cis</i>-Bis(2,2′-bipyridyl)bis(trifluoromethanesulfonato)cobalt(II)

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  • TOYAMA Mari
    Department of Chemistry of Functional Molecules, Faculty of Science and Engineering, Konan University
  • YAMAMOTO Yu
    Department of Chemistry of Functional Molecules, Faculty of Science and Engineering, Konan University

書誌事項

公開日
2019-04-10
DOI
  • 10.2116/xraystruct.35.21
公開者
社団法人 日本分析化学会

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説明

<p>A cobalt(II) complex with two 2,2′-bipyridine (bpy) and two trifluoromethanesulfonato (OTf−) ligands, cis-[CoII(OTf )2(bpy)2], was prepared, and the crystal structure at 173 K was elucidated by the single-crystal X-ray diffraction method. The complex crystallized in the monoclinic space group C2/c with a = 9.90587(16), b = 14.2978(2), c = 18.6626(3)Å, α = 90, β = 101.6670(17), γ = 90°, Z = 4, V = 2588.61(7)Å3. The R1 and wR2 values were 0.0397 and 0.1016, respectively, for 2377 reflections.</p>

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