Three-Dimensional Observation of Dislocation Structure by FIB-SEM
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- Yamasaki Shigeto
- 九州大学大学院工学研究院材料工学部門
Bibliographic Information
- Other Title
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- FIB-SEMによる転位組織の三次元観察
Description
<p>Three-dimensional visualization of dislocations by serial sectioning of SEM-ECCI images was performed on a creep-deformed nickel-based heat-resistant alloy. By performing serial tomograms of ECCI images, a volume of approximately 5 μm × 5 μm × 0.3 μm volume was successfully reconstructed. By incorporating the crystal orientation information obtained by the SEM-EBSD method, we confirmed that the three-dimensional arrangement of dislocations, such as slip planes and cross-slip, is accurately reflected in the three-dimensional volume. Thus, serial sectioning of ECCI images enables us to observe and analyze the bulk dislocation microstructure in three dimensions in the micrometer scale range.</p>
Journal
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- KENBIKYO
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KENBIKYO 58 (3), 90-94, 2023-12-30
The Japanese Society of Microscopy
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Details 詳細情報について
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- CRID
- 1390298753794987520
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- ISSN
- 24342386
- 13490958
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- Text Lang
- ja
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- Data Source
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- JaLC
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- Abstract License Flag
- Disallowed