Synthesis and Characterization of NMC 811 by Oxalate and Hydroxide Coprecipitation Method

DOI IR (HANDLE) Open Access
  • Himmah Sekar Eka Ayu Gustiana
    Chemical Engineering Department, Faculty of Vocational Studies, Universitas Sebelas Maret Centre of Excellence for Electrical Energy Storage Technology, Universitas Sebelas Maret
  • Firda Reza Agustiana
    Department of Physics Faculty of Mathematics and Natural Science, Universitas Sebelas Maret
  • Shofirul Sholikhatun Nisa
    Centre of Excellence for Electrical Energy Storage Technology, Universitas Sebelas Maret
  • Endah Retno Dyartanti
    Centre of Excellence for Electrical Energy Storage Technology, Universitas Sebelas Maret Chemical Engineering Department, Faculty of Engineering, Universitas Sebelas Maret

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Description

Synthesis of LiNi_0.8Mn_0.1Co_0.1O_2 (NMC 811) by coprecipitation method is promising for use. In this study, different precipitation agents were used to compar ing the characterization of each cathode. XRD analysis shows that both samples of NMC 811 have a highly layered hexagonal structure. By using FTIR analysis, it was indicated that the two cathodes contain C-H, O-H and C-O groups. Based on SEM analysis, the constituent particles of the cathodes are spherical asymmetrical with the size of the primary particle less than 1 micron and for the secondary particle more than 1 micron. The electrochemical performance showed that NMC-oxalate has a higher specific capacity than NMC -hydroxide. Based on this analysis, oxalate gave better results than hydroxide as a precipitate agent.

Journal

  • Evergreen

    Evergreen 9 (2), 438-442, 2022-06

    Transdiscilinary Research and Education Center for Green Technologies, Kyushu University

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Details 詳細情報について

  • CRID
    1390574257134936192
  • DOI
    10.5109/4794169
  • ISSN
    24325953
    21890420
  • HANDLE
    2324/4794169
  • Text Lang
    en
  • Article Type
    journal article
  • Data Source
    • JaLC
    • IRDB
    • Crossref
  • Abstract License Flag
    Allowed

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