Characterization of Crack Growth Acceleration of V-added Precipitation-strengthened High-Mn Austenitic Steel in High-pressure Gaseous Hydrogen Environment

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Other Title
  • 高圧水素環境におけるV添加析出強化型高Mnオーステナイト鋼のき裂進展加速機構

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<p>To verify the crack growth resistance of the V-added precipitation-strengthened high-Mn austenitic steel subject to a static and dynamic loading in a hydrogenated environment, the fracture toughness test and two types of fatigue crack growth (FCG) test, i.e., stress intensity factor range ΔK-increasing and ΔK-constant tests were performed under high-pressure gaseous hydrogen environment under the pressure of 95 MPa. The fracture toughness dramatically decreased from 95 to 35 MPa∙m1/2 by hydrogen occlusion. The fracture surface consists of intergranular fracture aspects in gaseous hydrogen despite being covered by the dimples tested in air. The FCG acceleration was also pronounced: more acceleration emerged as the ΔK became higher. When changing the loading frequency f as 1, 0.1, 0.01, and 0.001 Hz under constant ΔK of 30 MPa∙m1/2, the relative FCG rate in gaseous hydrogen to that in air became higher as f decreased, i.e., the dependency of FCG acceleration on the crack opening time. However, the acceleration did not completely depend on the crack opening time, which means a part of FCG acceleration was dominated by crack tip plasticity under cyclic loading. The scanning electron microscopy (SEM) characterization, including the electron-channeling contrast (ECC) imaging and the electron backscatter diffraction (EBSD) analysis, demonstrated that the crack preferentially propagates along grain boundary in the hydrogenated environment. The micro-void and/or micro-crack ahead of the primary FCG crack initiated at the M23C6 carbides precipitated at the grain boundary, which triggered the dramatic acceleration of FCG under 95 MPa gaseous hydrogen.</p>

Journal

  • Tetsu-to-Hagane

    Tetsu-to-Hagane 110 (16), 1288-1300, 2024-12-01

    The Iron and Steel Institute of Japan

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