Synthesis and reaction of N-methyl-N-phenylcarbamoyl chloride using microwaves

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  • マイクロ波を用いたN-メチル-N-フェニルカルバモイルクロリドの合成と反応
  • マイクロハ オ モチイタ N-メチル-N-フェニルカルバモイルクロリド ノ ゴウセイ ト ハンノウ

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Abstract

N-methy-N-phenylcarbamoyl chloride was synthsized by the reaction of N-methylformanilide and thionyl chloride under microwave irradiation. By the treatment of N-methyl-N-phenylcarbamoyl chloride with sodium ethoxide and N-methylaniline ethyl N-methyl-N-phenylcarbamate and N,N'-dimethyl N,N'-diphenylurea was obtained, respectively.

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