Total Synthesis of (+)‐Antimycin A<sub>3b</sub> on Solid Supports

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<jats:title>Abstract</jats:title><jats:p>A straightforward and convergent total synthesis of (+)‐antimycin A<jats:sub>3b</jats:sub> is reported. Four fragments were assembled on a solid support and the fully functionalized <jats:italic>seco</jats:italic> acid was cyclized in the solution phase. This synthetic route minimized the number of manipulations in the solution phase and is useful for a combinatorial library synthesis.</jats:p>

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