Unconventional Ligand‐to‐Catalyst Ratio for the Distal C−C Bond Formation via C−H Activation and Chain‐Walking

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説明

<jats:title>Abstract</jats:title><jats:p>A mechanism‐navigated enantioselective alkylation of an indole C2 C−H bond with an internal alkene was developed. Under the unconventional ligand‐to‐metal catalyst ratio, a moderate enantiomeric ratio (er), ranging from 70:30 to 88:12, was achieved with our original ligand. We propose that chain‐walking and bond formation are mechanistically independent and suggest that hydridoiridium generated from the C−H source does not play a role in the chain‐walking process.</jats:p>

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詳細情報 詳細情報について

  • CRID
    1870303266594410496
  • DOI
    10.1002/adsc.202400535
  • ISSN
    16154169
    16154150
  • データソース種別
    • OpenAIRE

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