Electrochemical preparation and reactions of unmasked acyl-anion synthons

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<jats:title>Abstract</jats:title><jats:p>1‐Pentyl bromide (I) is electroreductively coupled with pentacarbonyliron (II) to generate the acyliron compound (III) which is quenched with aqueous acid, forming heptanal (IV).</jats:p>

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