Fluoride‐Induced Chemiluminescent Decomposition of 1,2‐Dioxetanes (I) Bearing a Phenyl Moiety Substituted with a Methyl Having an Electron‐Withdrawing Group.

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A new type of dioxetane bearing a 3-(cyanomethyl)phenyl (1a), 3-(methoxycarbonylmethyl)phenyl (1b), 3-(benzoylmethyl)phenyl (1c), or 3-[cyano(methoxycarbonyl)methyl]phenyl group (1d) decomposed through an intermediary dioxetane bearing a benzylic carbanion to afford crimson to yellow light on treatment with TBAF in DMSO.

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