Structural studies of 2-, 3- and 4-pyridinecarboxylic acid methyl esters by gas-phase electron diffraction and 1H-NMR using a liquid crystal solvent

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書誌事項

タイトル
Structural studies of 2-, 3- and 4-pyridinecarboxylic acid methyl esters by gas-phase electron diffraction and 1H-NMR using a liquid crystal solvent
著者
Kiyono, Hajime
学位授与大学
北海道大学
取得学位
博士(理学)
学位授与番号
甲第4006号
学位授与年月日
1997-03-25

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説明

博士論文

資料形態 : テキストデータ プレーンテキスト
コレクション : 国立国会図書館デジタルコレクション > デジタル化資料 > 博士論文
博士論文

目次

3-4 Normal coordinate analysis

3-5 Analysis of electron diffraction data

3-6 Results and discussion

References

Appendix

Chapter 4 Structural study of methyl picolinate by gas electron diffraction combined with ab initio calculations

4-1 Introduction

4-2 Experimental

4-3 Ab initio calculations

4-4 Normal coordinate analysis

4-5 Analysis of electron diffraction data

4-6 Results and discussion

Chapter 5 Conformational studies by liquid crystal ¹H-NMR:methyl isonicotinate,methyl nicotinate and methyl picolinate

5-1 Introduction

5-2 Experimental

5-3 Analyses of NMR spectra

5-4 Vibrational corrections

5-5 Structural analyses

5-6 Results and discussion

Contents

Chapter 1 General introduction

1-1 Purpose of this study

1-2 Gas-phase electron diffraction

1-3 NMR using liquid crystal solvents

1-4 Chapters of this thesis

Chapter 2 Structural study of methyl isonicotinate by gas electron diffraction combined with ab initio calculations

2-1 Introduction

2-2 Experimental

2-3 Ab initio calculations

2-4 Normal coordinate analysis

2-5 Analysis of electron diffraction data

2-6 Results and discussion

Chapter 3 Structural study of methyl nicotinate by gas electron diffraction combined with ab initio calculations

3-1 Introduction

3-2 Experimental

3-3 Ab initio calculations

Chapter 6 Summary

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