Unique Synthetic Approach toward a Phosphaalkene: Synthesis of a Selenium-substituted Phosphaalkene with Bulky Substituents

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<jats:title>Abstract</jats:title> <jats:p>A selenium-substituted phosphaalkene, (Me3Si)2C=PSeTrp (1, Trp: 9-triptycyl), was synthesized by two methods, substitution reaction of (Me3Si)2C=PCl (3) with TrpSeLi, and treatment of TsiP(Cl)SeTrp (4, Tsi: C(SiMe3)3) with a catalytic amount of AlCl3. The newly obtained phosphaalkene was characterized in detail.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 43 (1), 95-96, 2013-10-09

    Oxford University Press (OUP)

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