Copper‐Catalyzed <i>sp</i><sup><i>3</i></sup>‐Carbon Radical/Halogen Radical Cross Coupling: Selective Halogenation of 1,3‐Dicarbonyl Compounds

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  • Shuai‐Shuai Lv
    Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Material Sciences Soochow University Suzhou, Jiangsu 215123 China
  • Xu‐Ping Yan
    Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Material Sciences Soochow University Suzhou, Jiangsu 215123 China
  • Cheng‐Kun Li
    Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Material Sciences Soochow University Suzhou, Jiangsu 215123 China
  • Shao‐Fang Zhou
    Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Material Sciences Soochow University Suzhou, Jiangsu 215123 China
  • Adedamola Shoberu
    Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Material Sciences Soochow University Suzhou, Jiangsu 215123 China
  • Jian‐Ping Zou
    Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry, Chemical Engineering and Material Sciences Soochow University Suzhou, Jiangsu 215123 China

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<jats:title>Abstract</jats:title><jats:p>A new copper‐catalyzed sp<jats:sup>3</jats:sup>‐carbon radical/halogen radical cross‐coupling strategy for the formation of C(sp<jats:sup>3</jats:sup>)‐X bond is described. This provides a general method for synthesis of <jats:italic>α</jats:italic>‐halogenated and <jats:italic>α</jats:italic>,<jats:italic>α</jats:italic>‐dihalogenated‐1,3‐dicarbonyl compounds using sodium halides as halogen source under mild conditions.</jats:p>

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