Cycloparaphenylene‐Based Ionic Donor–Acceptor Supramolecule: Isolation and Characterization of Li<sup>+</sup>@C<sub>60</sub>⊂[10]CPP

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公開日
2015-02-18
権利情報
  • http://onlinelibrary.wiley.com/termsAndConditions#vor
DOI
  • 10.1002/ange.201500544
  • 10.1002/anie.201500544
公開者
Wiley

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<jats:title>Abstract</jats:title><jats:p>The first cycloparaphenylene (CPP)‐based ionic donor–acceptor supramolecule Li<jats:sup>+</jats:sup>@C<jats:sub>60</jats:sub>⊂[10]CPP⋅X<jats:sup>−</jats:sup> has been synthesized. X‐ray crystallography not only confirmed the molecular structure of Li<jats:sup>+</jats:sup>@C<jats:sub>60</jats:sub>⊂[10]CPP⋅X<jats:sup>−</jats:sup> but also uncovered the formation of a unique ionic crystal. The strong charge‐transfer interaction between [10]CPP and Li<jats:sup>+</jats:sup>@C<jats:sub>60</jats:sub>, which was confirmed by electrochemical measurement and spectroscopic analyses, caused significant delocalization of the positive charge across the entire complex.</jats:p>

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