Solvent-Induced Controllable Synthesis, Single-Crystal to Single-Crystal Transformation and Encapsulation of Alq3 for Modulated Luminescence in (4,8)-Connected Metal–Organic Frameworks

  • Ya-Qian Lan
    National Institute of Advanced Industrial Science and Technology (AIST), Ikeda, Osaka 563-8577, Japan
  • Hai-Long Jiang
    National Institute of Advanced Industrial Science and Technology (AIST), Ikeda, Osaka 563-8577, Japan
  • Shun-Li Li
    Faculty of Chemistry, Northeast Normal University, Changchun 130024, P. R. China
  • Qiang Xu
    National Institute of Advanced Industrial Science and Technology (AIST), Ikeda, Osaka 563-8577, Japan

書誌事項

公開日
2012-06-26
DOI
  • 10.1021/ic202635a
公開者
American Chemical Society (ACS)

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説明

In this work, for the first time, we have systematically demonstrated that solvent plays crucial roles in both controllable synthesis of metal-organic frameworks (MOFs) and their structural transformation process. With solvent as the only variable, five new MOFs with different structures have been constructed, in which one MOF undergoes solvent-induced single-crystal to single-crystal (SCSC) transformation that involves not only solvent exchange but also the cleavage and formation of coordination bonds. Particularly, a significant crystallographic change has been realized through an unprecedented three-step SCSC transformation process. Furthermore, we have demonstrated that the obtained MOF could be an excellent host for chromophores such as Alq3 for modulated luminescent properties.

収録刊行物

  • Inorganic Chemistry

    Inorganic Chemistry 51 (14), 7484-7491, 2012-06-26

    American Chemical Society (ACS)

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