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- Zhang Yao
- Department of Natural Medicinal Chemistry, China Pharmaceutical University
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- Wang Jun-Song
- Department of Natural Medicinal Chemistry, China Pharmaceutical University
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- Luo Jun
- Department of Natural Medicinal Chemistry, China Pharmaceutical University
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- Kong Ling-Yi
- Department of Natural Medicinal Chemistry, China Pharmaceutical University
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抄録
Four novel nortriterpenoids, 24,25-epoxy-tirucall-7,20(E)-diene-3,23-dione (1), 24,25,26,27-tetranortirucall-1,7-diene-23(21)-lactone (2), 3α-hydroxy-tirucall-7-ene-20-one (3), and 3-oxo-tirucall-7-ene-3,20-dione (4), together with one known compound mombasol (5) were isolated from the stem barks of Aphanamixis grandifolia. Their structures were elucidated on the basis of various spectroscopic analysis including electrospray ionization (ESI)-MS, high resolution (HR)-ESI-MS, IR, 1D- and 2D-NMR techniques (heteronuclear single quantum coherence (HSQC), heteronuclear multiple bond connectivity (HMBC) and rotating frame Overhauser enhancement spectroscopy (ROESY)), and by comparison of their spectral data with those reported. The absolute configuration of compound 1 was determined by circular dichroism (CD) exciton chirality.
収録刊行物
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- CHEMICAL & PHARMACEUTICAL BULLETIN
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CHEMICAL & PHARMACEUTICAL BULLETIN 59 (2), 282-286, 2011
公益社団法人 日本薬学会
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詳細情報 詳細情報について
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- CRID
- 1390001204173109632
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- NII論文ID
- 130000405529
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- NII書誌ID
- AA00602100
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- ISSN
- 13475223
- 00092363
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- NDL書誌ID
- 10951954
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
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